2-(4-Methoxyphenyl)phenanthro[9,10-d]imidazole methanol solvate
نویسندگان
چکیده
The title compound, C(22)H(16)N(2)O·CH(4)O, is a product of the condensation reaction between phenanthrene-quinone and 4-methoxy-benzadehyde. There are two imidazole mol-ecules and two methanol molecules in the asymmetric unit. The phenanthryl and imidazole rings are almost parallel in both mol-ecules, with inter-planar angles of 6.65 (1) and 5.40 (3)°. The dihedral angles between the imidazole and the attached benzene rings are 5.40 (3) and 6.65 (1)° in the two molecules. Inter-molecular O-H⋯N and N-H⋯O hydrogen bonds stabilize the crystal packing.
منابع مشابه
Synthesis of tetra-substituted phenanthroimidazole derivatives using SBA-Pr-SO3H
A one pot four-component reaction of 9,10-phenanthraquinone, aromatic aldehyde, aniline, and ammonium acetate was designed for the preparation of tetrasubstituted imidazoles (phenanthro[9,10-d]imidazole) derivatives in the presence of SBA-Pr-SO3H as a mesoporous solid acid catalyst. Phenanthro[9,10-d]imidazole derivatives were produced by the use of this technique in short reaction times and go...
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